Allylmagnesium chloride 1.5M solution in THF
allylmagnesium chloride
CAS: 2622-05-1
Molecular Formula: C3H5ClMg
Allylmagnesium chloride 1.5M solution in THF - Names and Identifiers
| Name | allylmagnesium chloride |
| Synonyms | allylmagnesium chloride Allyl chlorideMagnesiuM ALLYLMAGNESIUM CHLORIDE chloro(prop-2-en-1-yl)magnesium Allylmagnesium chloride solution prop-2-en-1-ylmagnesium(1+) chloride ALLYLMAGNESIUM CHLORIDE, 2.0M SOLUTION I Allylmagnesium chloride 1.5M solution in THF ALLYLMAGNESIUM CHLORIDE SOLUTION, ~2.0 M IN THF ALLYLMAGNESIUM CHLORIDE, 2.0M SOLUTION I N TETRAHYDROFURAN |
| CAS | 2622-05-1 |
| EINECS | 220-067-1 |
| InChI | InChI=1/C3H5.ClH.Mg/c1-3-2;;/h3H,1-2H2;1H;/q;;+1/p-1/rC3H5Mg.ClH/c1-2-3-4;/h2H,1,3H2;1H/q+1;/p-1 |
| InChIKey | PLYLAFITHJUEGX-UHFFFAOYSA-M |
Allylmagnesium chloride 1.5M solution in THF - Physico-chemical Properties
| Molecular Formula | C3H5ClMg |
| Molar Mass | 100.83 |
| Density | 0.995g/mLat 25°C |
| Melting Point | -21°C |
| Boling Point | 66°C |
| Flash Point | 1°F |
| Water Solubility | vigorous reaction |
| Appearance | Liquid |
| Color | Clear tan to brown, amber, dark gray, dark green or black |
| BRN | 3587316 |
| Storage Condition | water-free area |
| Sensitive | Air & Moisture Sensitive |
Allylmagnesium chloride 1.5M solution in THF - Risk and Safety
| Risk Codes | R11 - Highly Flammable R14/15 - R34 - Causes burns R40 - Limited evidence of a carcinogenic effect R37 - Irritating to the respiratory system R19 - May form explosive peroxides |
| Safety Description | S16 - Keep away from sources of ignition. S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S43 - In case of fire use ... (there follows the type of fire-fighting equipment to be used.) S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) S7/8 - S6A - S43B - S33 - Take precautionary measures against static discharges. |
| UN IDs | UN 3399 4.3/PG 1 |
| WGK Germany | 1 |
| FLUKA BRAND F CODES | 1-3-10 |
| TSCA | Yes |
| HS Code | 29319090 |
| Hazard Class | 4.2 |
| Packing Group | I |
Allylmagnesium chloride 1.5M solution in THF - Reference Information
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| Overview | Allyl magnesium chloride is an organometallic compound and can be used as an intermediate in organic synthesis. |
| preparation | allyl magnesium chloride is prepared as follows: 20g of allyl chloride, 12vol THF are added to the allyl halogenated alkane supply device 11, shake well, and the obtained mixture is ready for use. The external bath temperature of the Grignard reagent preparation device 13 was raised to 50-55°C, and the mixture was pumped into the Grignard reagent preparation device 13. Under constant stirring, the magnesium chips are added from the metallic magnesium supply device 12 (solid feed funnel), and 0.4g I2 is added to the Grignard reagent preparation device 13 for thermal initiation. After thermal initiation, the temperature of the reaction system is immediately reduced to between 0 ~-15 ℃, a continuous Grignard reaction is carried out, and allyl magnesium chloride is continuously prepared. |
| use | Grignard reagent |
Last Update：2024-04-09 02:00:05
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Allylmagnesium chloride 1.5M solution in THF
4-THIAZOLEACETIC ACID, 2-AMINO-ALPHA-(METHOXYIMINO)-, (AZ)-, ANHYDRIDE WITH O,O-DIETHYL HYDROGEN PHOSPHOROTHIOATE
Ruthenium(II) chloride
BIS-TRIS HYDROCHLORIDE
4-AMINOMETHYLPIPERIDINE, BOC PROTECTED
3-丁氧基-2,4,6-三氟苯基硼酸
1330763-78-4
芴甲氧羰酰基Β环己基丙氨
4-{[4-(trifluoromethoxy)phenyl]methoxy}aniline
CHEMBL352955
4-THIAZOLEACETIC ACID, 2-AMINO-ALPHA-(METHOXYIMINO)-, (AZ)-, ANHYDRIDE WITH O,O-DIETHYL HYDROGEN PHOSPHOROTHIOATE
Ruthenium(II) chloride
BIS-TRIS HYDROCHLORIDE
4-AMINOMETHYLPIPERIDINE, BOC PROTECTED
3-丁氧基-2,4,6-三氟苯基硼酸
1330763-78-4
芴甲氧羰酰基Β环己基丙氨
4-{[4-(trifluoromethoxy)phenyl]methoxy}aniline
CHEMBL352955